![Single Crystal X-ray Diffraction Single Crystal X-ray Diffraction](/5242223/header_image-1417159667.jpg?t=eyJ3aWR0aCI6ODQ4LCJmaWxlX2V4dGVuc2lvbiI6ImpwZyIsIm9ial9pZCI6NTI0MjIyM30%3D--6207e0e5c0ef8586fc1d2295831143fb3913712d)
Single Crystal X-ray Diffraction
Equipment
Bruker AXS Smart APEX I:
- Three circle diffractometer with molybdenum X-ray tube.
- High sensitive 4k Chip: Maximum 2theta 78° / single frame.
- Measuring range: Maximum 2theta 150°.
- Low temperature device: Cryostream Plus, Oxford Cryosystems, temperature range 80 - 500 K.
- Software for evaluation and analysis of any kind of twinned crystals.
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Bruker AXS Smart APEX II + Incoatec IµS:
- Three circle diffractometer with conventional X-ray tube
(Mo) and Incoatec Microfocus Source IµS (Cu), changeable use. - High sensitive 4k Chip: Maximum 2theta 78° / single frame.
- Measuring range: Maximum 2theta 145° (Cu), 120° (Mo).
- Low temperature device: N-Helix, Oxford Cryosystems, temperature range 28 - 300 K.
- Video system for precise measuring of crystals (numerical absorption correction).
- Software for evaluation and analysis of modulated structures (commensurable and incommensurable).
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Application:
Structural characterisation of new compounds with the help of X-ray diffraction methods on single crystals: Measurements of samples sensitive to air and moisture. Low temperature investigations for analysis of phase transitions, structure determination of temperature sensitive compounds, investigation of aperiodic structures and complex twinned crystals.